浙江大學(xué)化學(xué)系研究生導(dǎo)師:吳金龍

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浙江大學(xué)化學(xué)系研究生導(dǎo)師:吳金龍

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浙江大學(xué)化學(xué)系研究生導(dǎo)師:吳金龍 正文


  姓名:吳金龍
  單位:化學(xué)系
  職稱:副教授

  基本信息
  個(gè)人簡(jiǎn)介
  學(xué)習(xí)簡(jiǎn)歷:
  1978年10月-1982年7月杭州大學(xué),理學(xué)學(xué)士;
  1986年9 月-1989年7月杭州大學(xué),理學(xué)碩士;
  1994年9 月-1997年6月杭州大學(xué)(1996年6月-1997年3月香港科技大學(xué)),理學(xué)博士。

  工作簡(jiǎn)歷:
  1982年8月-1986年8月水電部華東勘測(cè)設(shè)計(jì)院;
  1989年9月-1992年7月杭州有機(jī)硅新材料研究所,工程師;
  1992年8月-1994年8月杭州國(guó)森化學(xué)工業(yè)有限公司;
  1997年9月-1999年6月浙江大學(xué),博士后;
  1999年6月至今 浙江大學(xué),博士后出站后留校工作,從事有機(jī)化學(xué)的教學(xué)與研究工作.

  出國(guó)(境)進(jìn)修情況:
  199606-199703,200902-200908 香港科技大學(xué)

  工作研究領(lǐng)域
  研究領(lǐng)域:
  1.水相中有機(jī)反應(yīng)的研究;
  2.可控溫、控壓微波輻射條件下的快速、高效有機(jī)合成方法的研究;
  3.天然生物活性復(fù)雜大分子的全合成研究;
  4.自由基自旋捕捉劑的合成及應(yīng)用研究;
  5.藥物合成與開(kāi)發(fā),雜質(zhì)分離和結(jié)構(gòu)測(cè)定。

  聯(lián)系方式
  電話:86-571-87953128
  電子信箱:wyz@zju.edu.cn

  教學(xué)工作
  1.高等有機(jī)化學(xué)(博士研究生)
  2.有機(jī)合成(博士、碩士研究生)
  3.有機(jī)化學(xué)(甲)(本科生)
  4.有機(jī)化學(xué)(乙)(本科生)
  5.有機(jī)化學(xué)(丙)(本科生)
  6.大學(xué)化學(xué)實(shí)驗(yàn)(O)(本科生)
  7.有機(jī)化學(xué)(本科生)
  8.有機(jī)化學(xué)實(shí)驗(yàn)(本科生,生物求是科學(xué)班)

  工作研究項(xiàng)
  基金項(xiàng)目:
  1.[12]Cytochalasins類大環(huán)內(nèi)酯天然產(chǎn)物的全合成研究(國(guó)家自然科學(xué)基金項(xiàng)目 21172191 201201-201512,負(fù)責(zé)人)
  2.微波輔助Wittig-Diels-Alder串聯(lián)反應(yīng)的研究(國(guó)家自然科學(xué)基金項(xiàng)目 20572092,200601-200812,負(fù)責(zé)人)
  3.1,3-雙官能團(tuán)化合物合成及在立體選擇合成中的應(yīng)用(國(guó)家自然科學(xué)基金項(xiàng)目 20272050,200301-200512,參加)
  4.自旋探針的設(shè)計(jì)合成及在腫瘤早期診斷和干預(yù)中的應(yīng)用研究(浙江省自然科學(xué)基金 Y404302,200801-201012,負(fù)責(zé)人)
  5.微波輔助的水相Wittig反應(yīng)和芳香胺化醚化反應(yīng)及應(yīng)用研究( 浙江省自然科學(xué)基金 Y207295,200501-200612,負(fù)責(zé)人)

  企業(yè)項(xiàng)目:
  1.纈沙坦的產(chǎn)業(yè)化開(kāi)發(fā)研究(企業(yè)項(xiàng)目 2009,負(fù)責(zé)人)
  2.仿制原料藥及中間體的合成(企業(yè)項(xiàng)目 2008,參加)
  3.氧氟頭孢(Flomoxef)的合成研究(企業(yè)項(xiàng)目 2002,負(fù)責(zé)人)
  4.頭孢布烯(Ceftibuten)的合成(企業(yè)項(xiàng)目 1999,負(fù)責(zé)人)
  5.蒽環(huán)類抗腫瘤藥-4-去甲氧基柔紅霉素鹽酸鹽的合成研究(企業(yè)項(xiàng)目 1998,參加)

  發(fā)表論文
  54.Towards a Total Synthesis of Divergolides A: Synthesis of Amido Hydroquione Core and The C10-C15 Fragment: Guanglian Zhao, Jinlong Wu, and Wei-Min Dai, Synlett 2012, 2845-2849. [DOI: 10.1055/s-0032-1317491].
  53.Jing Dai, Jinlong Wu, Guanglian Zhao, and Wei-Min Dai, In(OTf)3-Catalyzed Highly Chemo- and Regioselective Head-to-Tail Hetereodimerization of Vinylarenes with 1,1-Diarylethenes Chem. Eur. J. 2011, 8290-8293. [DOI: 10.1002/chem.201101190].
  52.Yunxin Liu, Gaofeng Feng, Jian Wang, Jinlong Wu, and Wei-Min Dai, Synthesis of Two Diastereoisomers of Iriomoteolide-1a via a Tunable Four-Module Coupling Approach Using Ring-Closing Metathesis as the Key Step Synlett 2011, 1774-1778. [DOI: 10.1055/s-0030-1260822].
  51.Dongdong Wu, Huoming Li, Jian Jin, Jinlong Wu, and Wei-Min Dai Total Synthesis of Amphidinolide T3 Using Ring-Closing Metathesis and Asymmetic Dihydrolation Strategy Synlett 2011, 895-898 [DOI: 10.1055/s-0030-1259706].
  50.Jinlong Wu, Xiuqing Jiang, Jingjing Xu, and Wei-Min Dai Tandem Wittig-Intramolecular Diels-Alder Cycloaddition of Ester-Tethered 1,3,9-Decatrienes under Microwave Heating Tetrahedron, 2011, 67, 179-192. [DOI: 10.1016/j.tet.2010.10.088].
  49.Huoming Li, Jinlong Wu, Jialu Luo, and Wei-Min Dai, A Concise Total Synthesis of Amphidinolide T2: Chem. Eur. J. 2010, 16, 11530-11534. [DOI: 10.1002/chem.201001794].
  48.Yuanxin Liu, Jian Wang, Huoming Li, Jinlong Wu, Gaofeng Feng, and Wei-Min Dai, Synthesis of the C7–C23 Fragment Related to Iriomoteolide-1a via B-Alkyl Suzuki–Miyaura Cross-Coupling and Indium-Mediated Aldehyde Allylation: Synlett 2010, 2184-2188. [DOI: 10.1055/s-0030-1258507].
  47.Yu Zheng, Gongli Yu, Jinlong Wu, and Wei-Min Dai, Synthesis of N-Arylisoindolin-1-ones via Pd-Catalyzed Intramolecular Decarbonylative Coupling of N-(2-Bromobenzyl)oxanilic Acid Phenyl Esters: Synlett, 2010, 1075–1080. [DOI: 10.1055/s-0029-1219580].
  46.Yan Wang, Jinlong Wu, and Wei-Min Dai Stereoselectivity of Intramolecular Diels–Alder Reaction of Hydroxamate-Tethered 1,3,9-Decatrienes under Thermal and Microwave Heating: Synlett 2009, 2862–2866.
  45.Liang Sun, Jinlong Wu, and Wei-Min Dai Synthesis of C18–C28 Ketone Fragment of Micromonospolide B Possessing 1,3-Diene and 1,3-Anti-diol Functionalities: Tetrahedron: Asymmetry 2009, 20, 1864–1870.
  44.Jialu Luo, Huoming Li, Jinlong Wu, Xinglong Xing, and Wei-Min Dai Synthesis of the C1–C12 Acid Fragment of Amphidinolide T Marine Macrolides via SmI2-Mediated Enantioselective Reductive Coupling of Aldehydes with a Chiral Crotonate: Tetrahedron 2009, 65, 6828–6833.
  43.Liang Sun, Gaofeng Feng, Yucui Guan, Yuanxin Liu, Jinlong Wu, and Wei-Min Dai Influence of Appended Groups on Formation of 16-Membered Macrolactone Core Related to the Plecomacrolides via Diene–Ene Ring-Closing Metathesis: Synlett 2009, 2361–2365.
  42.Jinlong Wu, Yong Jiang, and Wei-Min Dai Assembly of 1,3-Dihydro-2H-3-benzazepin-2-one Conjugates via Ugi Four-Component Reaction and Palladium-Catalyzed Hydroamidation: Synlett 2009, 1162-1166. [DOI:10.1055/s-00280108815]. [DOI: 10.1055/s-0028-1088115].
  41.Wei-Min Dai, Jianyu Shi, Jinlong Wu, Synthesis of 3- Arylideneindolin- 2-ones from 2-Aminophenols by Ugi Four-Component Reaction and Heck Carbocyclization: Synlett, 2008, 2716-2720. [DOI: 10.1055/s-0028-1083505].
  40.鄧旭芳,劉珊林,施冬云,李浩然,吳金龍,黃勇超,自旋探針苯基-N-叔丁基硝酮納米粒的制備及其對(duì)肝腫瘤細(xì)胞的親和性研究藥學(xué)學(xué)報(bào),2008,43,308-313。
  39.Jinlong Wu, Yu Liao, Shanlin Liu N-[2-(2-Methoxyphenyl)benzylidene]-tert-Butylamine N-oxide Acta. Cryst. 2008, E64, o1099.
  38.Wei-Min Dai, Yile Chen, Jian Jin, Jinlong Wu, Jianshu Lou, Qiaojun He, Total Synthesis of Amphidinolide X and (12Z)-Isomer by Formation of the C12-C13 Trisubstituted Double Bond via Ring-Closing Metathesis. Synlett, 2008, 1737-1741.
  37.Wei-Min Dai, Yannian Li, Ye Zhang, Congyong Yue, Jinlong Wu, Generation of an Aromatic Amide-Derived Phosphine (Aphos) Library via Self-Assisted Molecular Editing and Screening for Suzuki-Miyaura Cross-Coupling of Unactivated Aryl Chlorides under Controlled MicroWave Heating: Chem. Eur. J. 2008, 14, 5538-5554.
  36.Wei-Min Dai, Gaofeng Feng, Jinlong Wu, and Liang Sun Synthesis of C3–C12 Fragment of 24-Demethylbafilomycin C1 via Anti-Selective Aldol Condensation as the Key Stereocontrol Step Synlett. 2008, 1013-1016.
  35.Jinlong Wu, Liang Nie, Jialu Luo and Wei-Min Dai Microvave-Assisted Pd-Catalyzed Intramolecular Direct Arylation for Synthesis of Novel Fused Heterocycles Synlett. 2007, 2728-2732.
  34.Jie Yan, Jinlong Wu and Hongwei Jin An efficient synthesis of diynes using (diacetoxyiodo)- benzene J. Organomet. Chem. 2007, 692, 3636-3639.
  33.Jinlong Wu, Haihua Yu, Yan Wang, Xinglong Xing, and Wei-Min Dai Unexpected Epimerization and Stereochemistry Revision of IMDA Adducts from Sorbate-Related 1,3,8-Nonatrienes Tetrahedron Lett. 2007, 48, 6543-6547.
  32.Jian Jin, Yile Chen, Yannian Li, Jinlong Wu, and Wei-Min Dai Total Synthesis of Amphidinolide Y by Formation of Tri-substituted (E)-Double Bond via RCM of Densely Functionalized Alkenes Org. Lett. 2007, 9, 2585-2588.
  31.Yucui Guan, Jinlong Wu, Liang Sun, and Wei-Min Dai Synthesis of C13-C25 Fragment of 24-Demethylbafilomycin C1 via Diastereoselective Aldol Reactions of a ketone Boron Enolate as the Key Step J. Org. Chem. 2007, 72, 4953-4960.
  30.Gaofeng Feng, Jinlong Wu, and Wei-Min Dai Isolation and Characterization of 2-Alkylaminobenzo[b]furans. Evidence for Competing O-Arylation in Cu-Catalyzed Intramolecular Amidation: Tetrahedron Lett. 2007, 48, 401-404.
  29.Xinglong Xing, Jinlong Wu, andWei-Min Dai Acid-Mediated Three-Component Aza-Diels-Alder Reactions of 2-Aminophenols under Controlled Microwave Heating for Synthesis of Highly Functionalized Tetrahydroquinolines: Tetrahedron 2006, 62, 11200-11206.
  28.Jin-Long Wu (aR,1R,2S,5R)-5-Methyl-2-(1-methyl-1-Phenylethyl)cyclohexyl (4-tert- Butylcyclohexylidene)acetate Acta Cryst. 2006, E62, o2967-o2968.
  27.Jinlong Wu, Lijie Sun, and Wei-Min Dai Microwave-Assisted Tandem Wittig-Intramolecular Diels- Alder Cycloaddition. Product Distribution and Stereochemical Assignment Tetrahedron 2006, 62, 8360-8372.
  26.Xinglong Xing, Jinlong Wu, Jialu Luo, and Wei-Min Dai C-N Bond-Linked Conjugates of Dibenz[b,f] [1,4]oxazepines with 2-Oxindole Synlett 2006, 2099-2103.
  25.Xinglong Xing, Jinlong Wu, Gaofeng Feng, and Wei-Min Dai Microwave-Assisted One-Pot U- 4CR and Intramolecular O-Alkylation toward Heterocyclic Scaffolds Tetrahedron 2006, 62, 6774-6781.
  24.Jinlong Wu and Congyong Yue“One-Pot” Wittig Reactions in Aqueous Media: A Rapid and Environmentally Benign Synthesis of a,b Unsaturated Carboxylic Esters and Nitriles Synth. Commun. 2006, 36, 2939-2947.
  23.Yile Chen, Jian Jin, Jinlong Wu, and Wei-Min Dai A New Synthesis ofTetrahydrofuran Fragment of Amphidinolides X and Y Synlett 2006, 1177-1180.
  22.Gaofeng Feng, Jinlong Wu, and Wei-Min Dai One-Pot Regioselective Annulation toward 3,4-Dihydro-3-oxo-2H-1,4-benzoxazine Scaffolds under Controlled Microwave Heating Tetrahedron 2006, 62, 4635-4642.
  21.Jinlong Wu, Dan Li, Huafeng Wu, Lijie Sun, and Wei-Min Dai Microwave-Assisted Regioselective Olefinations of Cyclic Mono- and Di-ketones with a Stabilized Phosphorus Ylide Tetrahedron 2006, 62, 4643-4650.
  20.Jinlong Wu, Dan Li and Da Zhang Aqueous Wittig Reactions of Aldehydes with in situ Formed Semi-Stabilized Phosphorus Ylides Synth.Commun. 2005, 35, 2543-2551.
  19.Jinlong Wu, Da Zhang and Shaoyong Wei Wittig reactions of stabilized phosphorus yildes with aldehydes in water Synth. Commun. 2005, 35, 1213-1222.
  18.Jinlong Wu, Huafeng Wu, Shaoyong Wei, and Wei-Min Dai Highly regioselective Wittig reactions of cyclic ketones with a stabilized phosphorus ylide under controlled microwave heating, Tetrahedron Lett., 2004, 45, 4401-4404
  17.Wei-Min Dai, Yannin Li, Ye Zhang, Kwong Wah Lai, and Jinlong Wu A novel class of amide-derived air-stable P, O-ligands for Suzuki cross-coupling at low catalyst loading Tetrahedron Lett. 2004, 45, 1999- 2001.
  16.魏少勇,吳金龍 無(wú)介質(zhì)微波作用下酮與穩(wěn)定葉立德的反應(yīng) 浙江大學(xué)學(xué)報(bào)(理學(xué)版),2003, 30 , 430-433
  15.Bing Zheng, Jin Long Wu, Shao Jun Xu, Jian Feng Shi, Yao Zu Chen, A Facile and Highly Stereoselective Reductive Debromination of Anhydro-6-(R)-Hydroxyethyl-6-Bromopenicillin, Chinese. Chem. Lett., 2000, 11, 385~386.
  14.Feng Lin, Jinlong Wu, Jiageng Liu, The study of far UV Irradiation of 2 -Methoxy-cytosine in Phosphate Solution and its Novel Photoproduct, J. Photochem. Photobio. A-Chem., 2000, 131, 49-53.
  13.Feng Lin, Jinlong Wu, Xiao-Wei Fan, A Novel Photoproduct of 2 -Methoxycytosine in Phosphate Solution under Far UV Irradiation,Chinese Chem. Lett., 1999, 623-624.
  12.Wei-Min Dai, Jinlong Wu, Kin Chiu Fong, Mavis Yuk Ha Lee, and Chi Wai Lau, Regioselective Synthesis of Acyclic cis-Enediynes via an Acid-Catalyzed Rearrangement of 1,2-Dialkynylallyl Alcohols. Syntheses, Computational Calculations and Mechanism. J. Org. Chem., 1999, 64, 5062-5082.
  11.Wei-Min Dai, Jinlong Wu, Anxin Wu, Two Distinct Epoxide Ring Oppening Pathways in a Monocyclic Model System of the Kedarcidin Chromophore; Tetrahedron Lett. 1998, 39, 4091-4094.
  10.Wei-Min Dai, Jinlong Wu, Xian Huang, Asymmetric Wittig Reaction of Chiral Arsonium Ylides 1. Asymmetric Olefination of 4-Substituted Cyclohexanones, Tetrahedron: Asymmetry, 1997, 8, 1979-1982.
  9.Wei-Min Dai, Jinlong Wu Stereoselective Synthesis of (Z)-Ketoeneyne via Pd(0)-Cu(I)-Catalyzed Cross-Couppling of (Z)-Ketoenoltriflate with 1-Alkynes, Tetrahedron, 1997, 53, 9107-9114.
  8.Xian Huang, Jinlong Wu Arylation of Allyl Cinnamyl and Propargyl Bromide with Triarylbismuth Catalyzed by Pd(0), Chinese Chem. Lett., 1997, 759-762.
  7.黃憲,吳露玲,杜敬星,吳金龍,黃志真,相轉(zhuǎn)移條件下亞烴基丙二酸亞異丙酯的鈀催化還原反應(yīng),杭州大學(xué)學(xué)報(bào)(自然科學(xué)版),1997,24,51.
  6.黃憲,吳金龍,2-烴基戊二酸酯的簡(jiǎn)便合成方法,有機(jī)化學(xué),1991,11,207-209
  5.黃憲,吳金龍,5-單取代亞烴基丙二酸亞異丙酯的簡(jiǎn)便合成方法,高等學(xué)?;瘜W(xué)學(xué)報(bào),1990,11,1388-1390。
  4.Xian Huang, Jinlong Wu A Facile Synthesis of 5-Mono-substituted Isopropylidene Malonate, Chem. J. Chinese Univ. (Series B), 1990, 6, 439.
  3.Xian Huang, Jinlong Wu Palladium Catalyzed Carbonylation of Aromatic Halides under PTC Condition, Chemistry and Industry 1990, 548.
  2.陳立佛,吳金龍,王均環(huán) 四氟乙烯齊聚體的反應(yīng)IV-四氟乙烯四及五聚體和芳香胺的反應(yīng),化學(xué)學(xué)報(bào),1984,42,470。
  1.陳立佛,吳金龍,王均環(huán) 四氟乙烯齊聚體的反應(yīng):四氟乙烯四、五聚體和芳香胺的反應(yīng),化學(xué)學(xué)報(bào),1983,41,668-671。

  出版著作
  1.新編有機(jī)合成化學(xué) 20030101

  專利成果
  1.一種合成肉桂酰胺類化合物的方法;吳金龍,岳從永,戴偉民;200510060207.9,2005年7月29日;CN1740145A,2006年3月1日;ZL 2005 1 0060207.9,2007年5月9日.
  2.紅景天苷的一種化學(xué)合成方法;吳金龍,廖宇,劉珊林;200610053035.7,2006年8月21日;CN1911949A,2007年2月14日;ZL 2006 1 0053035.7,2008年10月22日.
  3.α-聯(lián)苯基-N-烷基硝酮類化合物及其合成方法;吳金龍,廖宇,戴靜,朱明江,劉珊林;200810059423.5,2008年01月21日;CN101225056A,2008年07月23日.
  4.a(chǎn)-聯(lián)苯硝酮類碳環(huán)卡賓-鈀絡(luò)合物及其合成方法;吳金龍,戴靜,戴偉民;200810061133.4,2008年3月11日;CN101250202A,2008年8月27日;ZL 2008 1 0061133.4,2010年08月11日
  5.(E)-3-芳基-2-丙烯酰胺類化合物的合成方法;吳金龍,劉元鑫,戴偉民;200810061481.1,2008年5月5日;CN101274901A,2008年10月1日;ZL 2008 1 0061481.1,2010年06月23日.
  6.六氫異喹啉酮類化合物及其合成方法;吳金龍,趙健,戴偉民;200910100758.1,2009年7月21日;CN101602725A,2009年12月16日;ZL 2009 1 0100758.1,2012年7月11日
  7.六氫異吲哚類化合物及其合成方法;吳金龍,趙健,戴偉民;200910100757.7,2009年7月21日;CN101602705A,2009年12月16日.

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